Grafting time (h) | Elemental, % | Deconvolution, % | |||||
---|---|---|---|---|---|---|---|
C 1s | Ca 2p | ||||||
Graphitic carbon | CO | COO | COOR | Ca2C | Ca2C | CaO | |
8 | 42.77 | 39.08 | 18.15 | ND | ND | ND | ND |
16 | 35.35 | 37.38 | 27.28 | ND | ND | ND | ND |
24 | 26.49 | 58.96 | 8.62 | 5.94 | ND | ND | ND |
32 | 24.03 | 55.23 | 4.05 | 16.69 | ND | ND | ND |
48 | 43.26 | 33.87 | 12.68 | 10.19 | ND | ND | ND |
Raw CSAC | 77.80 | 14.18 | 8.20 | ND | ND | ND | ND |
Spent CMC-CSAC | 54.63 | 16.46 | 6.11 | ND | 22.81 | 27.37 | 72.63 |