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Table 3 The main condition of the scale-up electrolysis

From: Preparation of ursodeoxycholic acid from 7-ketone lithocholic acid by stereoselective electroreduction

Experiment 7K-LCA Methanol KBr H2O DMF Temperature
(kg) (kg) (kg) (kg) (kg) (°C)
1 6 280 2.7 24 6.5 55
2 6 280 2.7 24 6.5 45
3 6 280 2.7 20 6.5 45
4 6 280 2.7 20 6.5 55