Skip to main content

Table 1 1H NMR (600 MHz) and 13C NMR (150 MHz) results for silylated HOBB in DMSO-d 6

From: 2-Hydroxy-4-(3′-oxo-3′H-benzofuran-2′-yliden)but-2-enoic acid biosynthesis from dibenzofuran using lateral dioxygenation in a Pseudomonas putida strain B6-2 (DSM 28064)

δ (ppm)

Proton assignment

J (Hz)

δ (ppm)

Carbon assignment

6.468

H-9, d

3J = 12.2

106.32

C-10

6.698

H-10, d

3J = 12.2

112.26

C-9

7.065

H-4, t

3J = 7.4

113.91

C-2

7.231

H-2, d

3J = 8.2

122.32

C-6

7.518

H-3, t

3J = 7.4

124.81

C-4

7.543

H-5, d

3J = 7.3

125.07

C-3

   

138.54

C-5

   

147.69

C-8

   

148.76

C-11

   

163.92

C-12

   

165.82

C-1

   

183.42

C-7