Table 5 Experimental design matrix and the resulting yield
Run | Methanol/oil ratio (mol) | Catalyst load (wt%) | Reaction time (min) | Yield (%) |
|---|---|---|---|---|
1 | 4 | 0.75 | 60 | 94.48 |
2 | 4 | 0.75 | 60 | 92.37 |
3 | 5 | 0.55 | 45 | 91.88 |
4 | 3 | 0.55 | 45 | 95.52 |
5 | 4 | 0.75 | 60 | 93.13 |
6 | 4 | 0.75 | 60 | 93.68 |
7 | 4 | 0.75 | 60 | 94.47 |
8 | 5 | 0.95 | 75 | 88.74 |
9 | 5 | 0.55 | 75 | 94.64 |
10 | 6 | 0.75 | 60 | 88.26 |
11 | 2 | 0.75 | 60 | 93.97 |
12 | 3 | 0.95 | 45 | 93.41 |
13 | 5 | 0.95 | 45 | 88.78 |
14 | 3 | 0.95 | 75 | 89.12 |
15 | 4 | 1.15 | 60 | 87.23 |
16 | 4 | 0.75 | 30 | 93.74 |
17 | 4 | 0.35 | 60 | 96.17 |
18 | 4 | 0.75 | 60 | 93.92 |
19 | 3 | 0.55 | 75 | 95.27 |
20 | 4 | 0.75 | 90 | 92.69 |