Run no. (cluster no.) | Factors | Responses | Mass balance | ||||||
---|---|---|---|---|---|---|---|---|---|
X1, % | X2, min | X3, °C | X4, Mesh size | CNC yield, % | CSR yield, % | Total yield, % | Loss, % | Overall closure, % | |
1 (3) | 54 | 90 | 65 | 20 | 27.9 ± 1.3 | – | 27.9 ± 1.3 | 25.6 | 53.5 |
2 (3) | 66 | 30 | 65 | 20 | 25.2 ± 0.9 | – | 25.2 ± 0.9 | 29.2 | 54.4 |
3 (2) | 54 | 30 | 65 | 20 | 33.7 ± 2.8 | 22.0 ± 2.2 | 55.7 ± 0.6 | 18.6 | 74.3 |
4 (2) | 60 | 60 | 55 | 40 | 38.3 ± 2.9 | 16.9 ± 3.5 | 55.2 ± 0.6 | 18.5 | 73.7 |
5 (2) | 54 | 30 | 65 | 60 | 41.7 ± 1.9 | 20.7 ± 0.0 | 62.4 ± 1.9 | 10.4 | 72.8 |
6 (2) | 60 | 60 | 55 | 60 | 52.1 ± 3.3 | – | 52.1 ± 3.3 | 19.9 | 72.0 |
7 (1) | 66 | 30 | 45 | 20 | 20.1 ± 0.5 | 31.4 ± 0.6 | 51.5 ± 0.0 | 11.5 | 63.0 |
8 (2) | 60 | 90 | 55 | 40 | 51.6 ± 1.6 | – | 51.6 ± 1.6 | 15.9 | 67.5 |
9 (1) | 60 | 60 | 45 | 40 | 12.8 ± 0.4 | 62.3 ± 1.5 | 75.1 ± 1.2 | 6.3 | 81.4 |
10 (2) | 54 | 90 | 65 | 60 | 37.2 ± 1.1 | – | 37.2 ± 1.1 | 15.0 | 52.2 |
11 (1) | 60 | 30 | 55 | 40 | 29.5 ± 0.9 | 33.6 ± 3.9 | 63.0 ± 3.1 | 14.9 | 77.9 |
12 (1) | 54 | 60 | 55 | 40 | 23.2 ± 0.2 | 53.0 ± 2.6 | 76.2 ± 2.4 | 7.7 | 83.9 |
13 (3) | 66 | 30 | 65 | 60 | 15.0 ± 0.6 | – | 15.0 ± 0.6 | 34.8 | 49.8 |
14 (2) | 60 | 60 | 55 | 40 | 37.1 ± 1.6 | 20.8 ± 1.8 | 57.9 ± 0.2 | 15.0 | 72.9 |
15 (3) | 66 | 90 | 65 | 20 | 22.6 ± 0.3 | – | 22.6 ± 0.3 | 37.5 | 60.1 |
16 (3) | 66 | 60 | 55 | 40 | 17.3 ± 0.4 | – | 17.3 ± 0.4 | 43.6 | 60.9 |
17 (1) | 54 | 90 | 45 | 20 | 15.6 ± 0.4 | 59.6 ± 1.3 | 75.2 ± 0.9 | 4.4 | 79.6 |
18 (3) | 66 | 90 | 65 | 60 | 23.4 ± 0.8 | – | 23.4 ± 0.8 | 33.3 | 56.7 |
19 (2) | 60 | 60 | 55 | 20 | 38.0 ± 0.9 | 13.6 ± 0.3 | 51.5 ± 0.6 | 21.8 | 73.3 |
20 (3) | 66 | 30 | 45 | 60 | 18.0 ± 0.2 | – | 18.0 ± 0.2 | 23.5 | 41.5 |
21 (4) | 54 | 30 | 45 | 20 | 0.6 ± 0.1 | 83.3 ± 2.3 | 83.9 ± 2.3 | 1.6 | 85.5 |
22 (4) | 54 | 90 | 45 | 60 | 3.2 ± 0.0 | 77.7 ± 0.8 | 80.8 ± 0.8 | 3.5 | 84.3 |
23 (2) | 60 | 60 | 65 | 40 | 33.2 ± 1.3 | – | 33.2 ± 1.3 | 24.3 | 57.5 |
24 (4) | 54 | 30 | 45 | 60 | 1.1 ± 0.0 | 84.5 ± 1.0 | 85.6 ± 0.9 | 2.2 | 87.8 |
25 (3) | 66 | 90 | 45 | 20 | 11.9 ± 0.1 | – | 11.9 ± 0.1 | 40.5 | 52.4 |
26 (3) | 66 | 90 | 45 | 60 | 14.8 ± 0.3 | – | 14.8 ± 0.3 | 44.9 | 59.7 |