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Table 1 An overview of the sample preparation and Sc-CO2 parameters for fish oil and enzyme recovery

From: Sc-CO2 extraction of fish and fish by-products in the production of fish oil and enzyme

Sample

Particle size (µm)

Sample: CO2 mass ratio

Sc-CO2 parameter

Oil yield (%)

Protein yield/ Total protein

Enzyme activity

References

Pressure (MPa)

Temperature (°C)

Extraction time (min)

Flow rate (g/min)

Fish/ FBP oil, protein properties and enzyme recovery studies

Tuna viscera

250–1000

-

10.3–13.8

25–40

20–120

50

58–97

38–50%

NA

Kang et al.(2005)

Squid viscera

710

1:3

25

35–45

5–40

3

28–33

NM

NM

Park et al. (2006)

Mackerel viscera

710

1: 3

25

35–45

24

3

13–16

NM

Protease, lipase, amylase:

67.3- 84.1%

(Park et al. 2008)

Squid viscera

700

1:4

15–25

35–45

150

22

22–30

NM

Protease, lipase, amylase:

0.062 -0.4 U/ml

Uddin et al. (2009)

Starfish pyloric caeca

NM

1:4

25

40

150

28

NM

Phospholipase A2:

3978 mg/ml

Phospholipase A2: 100 U/mg

Chun et al., (2010)

Mackerel viscera

NM

1:4

25

45

150

28

NM

Trypsin: 1390 mg/ml

Trypsin: 0.8 U/mg

Chun et al. (2011)

Krill

700

1:2

15–25

35–45

150

22

NM

NM

Protease, lipase, amylase:

0.05–0.45 U/mg

Ali-Nehari et al. (2012)

Mackerel muscle

NM

1: 5

15–25

45

120

27

16–20

9.28 mg/ml

Lipase, protease, Trypsin, amylase: 8- 45 U/mg

Asaduzzaman & Chun (2015)

Gilthead sea bream

NM

-

25

45

240

167

NM

73 mg/ml

Proteolytic and Trypsin activity: 0.0057 & 0.0116 U/mg

Lamas (2015)

Fish/FBP oil studies

Brazilian redspotted shrimp waste (head, tail and shell)

331

1:20

30

50

20

5

2.21 (without co-solvent)

2.9 (with co-solvent)

49

NA

(Sánchez-Camargo et al. 2011)

Brazilian redspotted shrimp waste (cephalothoraxes, shells and tails)

331

1:20

30

50

100

3000

39.7- 93.8 (diff. co-solvent %)

NA

NA

(Sánchez-Camargo et al. 2012)

Catfish viscera

NM

1:1

10—40

35—80

60–240

1—3

47.5–67

NA

NA

(Sarker et al. 2012)

Carp viscera

NM

1:5

20–40

40–60

30–180

3–6

2.6–74.8

NA

NA

(Lisichkov et al. 2014)

Mackerel waste (skin (S), muscle tissue (F)), and viscera (V))

200–500

1:2

35

60

360

2

F,V,S: 20–43

NA

NA

(Hajeb et al. 2015)

Tuna waste (head (H), skin (S) and viscera (V))

500–1000

1: 2

40

65

120

3

H,S,V:

T. tonggol: 13.5–35.6

E. affinis: 16.1–28.4

A. thazard: 16.8–29.5

NA

NA

(Ferdosh et al. 2015)

Atlantic Salmon by-products ((belly part, trimmed muscle, frame bone and skin)

NM

1:1

25

45

180

27

76.21–86.99

NA

NA

(Haq et al. 2017)

Carp tissues: viscera (V), fillets (F) and caviar (C)

NM

1: 5

20–40

40–60

30–180

3

C,F,V: 8–51

NA

NA

(Kuvendziev et al. 2018)

  1. NA Not applicable, NM not mentioned; “- “: The sample: CO2 mass ratio could not be calculated due to insufficient information in the articles