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Table 3 Methods of conversion of chitin to chitosan

From: Seafood waste: a source for preparation of commercially employable chitin/chitosan materials

S. no

Method

Type of conditions

Deacetylation degree (%)

References

1.

Chemical

12.5 M NaOH (140 °C for 4 h)

 

Hajji et al. (2014)

2.

Chemical

Soaking in 18 M NaOH (24 h), Heating (90 °C for 7 h)

94.9

Ma et al. (2015)

3.

Chemical and microwave irradiation

50% NaOH, 8 min irradiation at 350 W

82.7

Knidri et al. (2016)

4.

Ultrasound-assisted chemical method

40% NaOH, alternate irradiation (45 min) and non-irradiation (30 min) periods

77.9

Birolli et al. (2016)

5.

Ultrasound-assisted chemical method

Ultrasound-assisted deacetylation chitin in 40% NaOH (50 min, 60 °C)

95

Fiamingo et al. (2016)

6.

Chemical

Soaking chitin in 50% NaOH and autoclaved

88

Sedaghat et al. (2017)

7.

Chemical

50% NaOH (90 °C, 30 h)

74

Yong et al. (2018)

  1. The physiochemical properties of chitin and chitosan have been summarized in Table 4